An in-vacuum x-ray diffraction microscope for use in the 0.7-2.9 keV range.

نویسندگان

  • D J Vine
  • G J Williams
  • J N Clark
  • C T Putkunz
  • M A Pfeifer
  • D Legnini
  • C Roehrig
  • E Wrobel
  • E Huwald
  • G van Riessen
  • B Abbey
  • T Beetz
  • J Irwin
  • M Feser
  • B Hornberger
  • I McNulty
  • K A Nugent
  • A G Peele
چکیده

A dedicated in-vacuum coherent x-ray diffraction microscope was installed at the 2-ID-B beamline of the Advanced Photon Source for use with 0.7-2.9 keV x-rays. The instrument can accommodate three common implementations of diffractive imaging; plane wave illumination; defocused-probe (Fresnel diffractive imaging) and scanning (ptychography) using either a pinhole, focused or defocused probe. The microscope design includes active feedback to limit motion of the optics with respect to the sample. Upper bounds on the relative optics-to-sample displacement have been measured to be 5.8 nm(v) and 4.4 nm(h) rms/h using capacitance micrometry and 27 nm/h using x-ray point projection imaging. The stability of the measurement platform and in-vacuum operation allows for long exposure times, high signal-to-noise and large dynamic range two-dimensional intensity measurements to be acquired. Finally, we illustrate the microscope's stability with a recent experimental result.

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عنوان ژورنال:
  • The Review of scientific instruments

دوره 83 3  شماره 

صفحات  -

تاریخ انتشار 2012